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Analyzing Residual Solvents in Pharmaceutical Products Using GC Headspace with Valve-and-Loop Sampling
Instrument Type: GCThis application note describes the analysis of residual solvents in accordance with USP method <467> using the Thermo Scientific™ TRACE™ 1310 GC, the new Thermo Scientific™ TriPlus™ 300 Headspace autosampler, and the Thermo Scientific™ Dionex™ Chromeleon™ chromatography data system (CDS) software. The method details the chromatographic system and analytical conditions to be used and addresses the acceptable limits for each solvent.
USP 467 analysis of residual solvents using GC-FID with headspace
Instrument Type: GCThe Thermo Scientific TRACE GC Ultra is applied for the analysis of residual solvents by USP method 467. The separation was performed on a Thermo Scientific TRACE TR-V1 GC column, with flame ionization detection.