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CAN122: Determination of Persistent Organic Pollutants in Fish Tissues by Accelerated Solvent Extraction and GC-MS/MS

Instrument Type: GCMSMS

Polychlorinated biphenyls (PCBs), organochlorine pesticides (OCPs) and polybrominated diphenyl ethers (PBDEs) belong to a broad family of synthetic organic compounds known as halogenated hydrocarbons. Polychlorinated biphenyls (PCBs), organochlorine pesticides (OCPs) and polybrominated diphenyl ethers (PBDEs) belong to a broad family of synthetic organic compounds known as halogenated hydrocarbons. The method reported here is applicable for the determination of 29 halogenated hydrocarbons (6 PCBs, 16 OCPs, and 7 PBDEs) in fish tissues.

CAN120: Determination of Total Petroleum Hydrocarbons in Rubble and Soils by Accelerated Solvent Extraction and GC-FID
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Instrument Type: GC

Recent advances in Accelerated Solvent Extraction systems, reduces the time spent on sample preparation prior to GC analysis. The method reported here is applicable to soils with a hydrocarbon content (HC)(>C12) between 25 and 4000 mg/kg and waste with a HC (C10-C40) between 50 and 8000 mg/kg expressed on a dry matter basis. All hydrocarbons with a boiling range of approximately 175 °C to 525 °C, e.g. n-alkanes from C10H22 to C40H82, isoalkanes, cycloalkanes, alkyl benzenes, alkyl naphthalenes, and polycyclic aromatic compounds are determined as total petroleum hydrocarbons (TPH).